Certificate of Analysis Agilent Part No. 8500-5440 Performance Evaluation Sample for GC/MS Systems Lot No. 462-75A Benzophenone Concentration Temperature Program Rate Injection Temperature Sample Size Column Flow Injection Mode SIM 100 pg/uL in Isooctane 90º(3 min) -> 250º 10ºC/min 250ºC Transfer Temperature 1.0 uL HP-5MS (30m x 0.25mm x 0.25um) 1.0 ml/min Pulsed Splitless 77, 105, 182 280ºC Abundance TIC: 7401005.D\ data.ms 12.557 7000 6500 6000 5500 5000 4500 4000 3500 3000 2500 2000 1500 1000 500 0 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 Time--> Area Percent Report Data File: Acq On Operator Sample ALS Vial Signal D:\msdchem\aug0911\7401005.D : 9 Aug 2011 10:58 : mbo : 8500-5440 Benzophenone : 74 : TIC: 7401005.D\data.ms peak R.T. first max last PK # min scan scan scan TY --- ----- ----- ---- ---- --1 12.557 1604 1623 1701 BB peak height ------6572 corr. corr. % of area % max. total ------- ------ ------285477 100.00% 100.000% Date of release: 9 August, 2011 Date of expiration: 9 August, 2014 John Conrad CSM/TC
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